L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate)

Base Information

Chemical Name:L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate)
CAS No.:81562-15-4
Molecular Formula:C₃₅H₄₀O₆S₂
Molecular Weight:620.831
Hs Code.:

Synonyms:L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate)

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Chemical Property of L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate)

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Technology Process of L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate)

There total 2 articles about L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 81562-15-4
L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate)

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / 5percent sodium hydroxide / tetrabutylammonium iodide / H₂O; CH₂Cl₂ / 48 h / Heating

2: 1.) 50percent sodium hydride, imidazole / 1.) THF, reflux, 5 h, 2.) THF, reflux, 1 h

With 1H-imidazole; sodium hydroxide; sodium hydride; tetra-(n-butyl)ammonium iodide; In dichloromethane; water;
DOI:10.1016/S0008-6215(00)81001-0

Reference yield:

: 13035-66-0
L-3,4-di-O-benzyl-1,2-O-cyclohexylidene-chiro-inositol

: 81562-15-4
L-1,3,4-tri-O-benzyl-5,6-O-cyclohexylidene-chiro-inositol 2-(S-methyl dithiocarbonate)

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / 5percent sodium hydroxide / tetrabutylammonium iodide / H₂O; CH₂Cl₂ / 48 h / Heating

2: 1.) 50percent sodium hydride, imidazole / 1.) THF, reflux, 5 h, 2.) THF, reflux, 1 h

With 1H-imidazole; sodium hydroxide; sodium hydride; tetra-(n-butyl)ammonium iodide; In dichloromethane; water;
DOI:10.1016/S0008-6215(00)81001-0