N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide

Base Information

• Chemical Name: N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide
• CAS No.: 861853-33-0
• Molecular Formula: C₄₈H₄₀Br₂N₂O₄
• Molecular Weight: 868.665

Synonyms:N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide

Chemical Property of N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide

There total 2 articles about N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

2,6-diisopropylbenzenamine (24544-04-5) + perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide (861853-33-0) + 1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide (331861-94-0)

Guidance literature:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride; With bromine;

2,6-diisopropylbenzenamine; With propionic acid; at 155 ℃; for 22h;

DOI:10.1021/jp1085334

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) + perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide (861853-33-0) + N,N’-di-(2,6-diisopropylphenyl)-1-bromoperylene-3,4:9,10-tetracarboxylic acid diimide (869276-74-4) + 1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide (331861-94-0)

Guidance literature:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride; With sulfuric acid; at 20 ℃; for 12h;

With iodine; at 20 - 85 ℃; for 0.5h;

2,6-diisopropylbenzenamine; Further stages;

DOI:10.1021/ol902526t

Reference yield: 95.0%

N,N'-bis(2,6-diisopropylphenyl)-1,6-dibromoperylene-3,4:9,10-tetracarboximide (861853-33-0) + C30H27NO4 (923584-43-4) + 1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide (331861-94-0) → C108H92N4O12 (923584-45-6) + C108H92N4O12 (923584-44-5)

Guidance literature:

With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 20h;

upstream raw materials:

2,6-diisopropylbenzenamine

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

Downstream raw materials:

N,N'-bis(2,6-diisopropylphenyl)-1,7-di(2,6-diisopropylphenoxy)perylene-3,4:9,10-tetracarboximide

N,N'-bis(2,6-diisopropylphenyl)-1,6-di(2,6-diisopropylphenoxy)perylene-3,4:9,10-tetracarboximide

C₁₀₈H₉₂N₄O₁₂

C₁₀₈H₉₂N₄O₁₂

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