5-(3-methyl-4-propoxybenzyl)-2-(methylsulfanyl)-4,6-pyrimidinediol

Base Information

Chemical Name:5-(3-methyl-4-propoxybenzyl)-2-(methylsulfanyl)-4,6-pyrimidinediol
CAS No.:332414-23-0
Molecular Formula:C₁₆H₂₀N₂O₃S
Molecular Weight:320.412
Hs Code.:
Mol file:332414-23-0.mol

Synonyms:2-methylthio-4,6-dihydroxy-5-(3-methyl-4-propoxybenzyl)pyrimidine

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Chemical Property of 5-(3-methyl-4-propoxybenzyl)-2-(methylsulfanyl)-4,6-pyrimidinediol

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Technology Process of 5-(3-methyl-4-propoxybenzyl)-2-(methylsulfanyl)-4,6-pyrimidinediol

There total 2 articles about 5-(3-methyl-4-propoxybenzyl)-2-(methylsulfanyl)-4,6-pyrimidinediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.1%

: 797806-29-2
2-mercapto-4,6-dihydroxy-5-(3-methyl-4-propoxybenzyl)pyrimidine

: 74-88-4
methyl iodide

: 332414-23-0
2-methylthio-4,6-dihydroxy-5-(3-methyl-4-propoxybenzyl)pyrimidine

Guidance literature:: 2-mercapto-4,6-dihydroxy-5-(3-methyl-4-propoxybenzyl)pyrimidine; With methanol; potassium hydroxide; for 0.166667h; Heating;

methyl iodide; In methanol; for 0.333333h; Heating;
DOI:10.1023/A:1010398911988

Reference yield:

: 355409-63-1
(3-methyl-4-propoxybenzyl)malonic acid diethyl ester

: 332414-23-0
2-methylthio-4,6-dihydroxy-5-(3-methyl-4-propoxybenzyl)pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 72.8 percent / EtONa / 8 h / Heating

2.1: KOH; MeOH / 0.17 h / Heating

2.2: 74.1 percent / methanol / 0.33 h / Heating

With methanol; potassium hydroxide; sodium ethanolate;
DOI:10.1023/A:1010398911988