Technology Process of 2-(9-Hydroxy-nonyl)-5,6-dimethoxy-3-methyl-phenol
There total 6 articles about 2-(9-Hydroxy-nonyl)-5,6-dimethoxy-3-methyl-phenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
methanol;
at 5 ℃;
for 24h;
Yield given;
DOI:10.1248/cpb.33.4422
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 93 percent / KMnO4, MgSO4*7H2O / acetone / 4 h / Ambient temperature
2: PCl5 / CH2Cl2 / 2 h / 25 °C
3: AlCl3 / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h
4: 78 percent / NaOH / methanol / 2 h / Ambient temperature
5: H2, 70percent HClO4 / 5percent Pd-C / 24 h / Ambient temperature
6: NaOH / methanol / 24 h / 5 °C
With
sodium hydroxide; potassium permanganate; aluminium trichloride; perchloric acid; phosphorus pentachloride; hydrogen; magnesium sulfate;
palladium on activated charcoal;
In
methanol; dichloromethane; 1,2-dichloro-ethane; acetone;
DOI:10.1248/cpb.33.4422
- Guidance literature:
-
Multi-step reaction with 5 steps
1: PCl5 / CH2Cl2 / 2 h / 25 °C
2: AlCl3 / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h
3: 78 percent / NaOH / methanol / 2 h / Ambient temperature
4: H2, 70percent HClO4 / 5percent Pd-C / 24 h / Ambient temperature
5: NaOH / methanol / 24 h / 5 °C
With
sodium hydroxide; aluminium trichloride; perchloric acid; phosphorus pentachloride; hydrogen;
palladium on activated charcoal;
In
methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422
