Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester

Base Information

• Chemical Name: Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester
• CAS No.: 77712-36-8
• Molecular Formula: C₂₀H₃₂O₅
• Molecular Weight: 352.471
• Mol file: 77712-36-8.mol

Synonyms:Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester

Chemical Property of Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester

There total 5 articles about Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-acetoxynonal (29541-97-7) → Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester (77712-36-8)

Guidance literature:

Multi-step reaction with 5 steps

1: 93 percent / KMnO₄, MgSO₄*7H₂O / acetone / 4 h / Ambient temperature

2: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

3: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

4: 78 percent / NaOH / methanol / 2 h / Ambient temperature

5: H₂, 70percent HClO₄ / 5percent Pd-C / 24 h / Ambient temperature

With sodium hydroxide; potassium permanganate; aluminium trichloride; perchloric acid; phosphorus pentachloride; hydrogen; magnesium sulfate; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane; acetone;

DOI:10.1248/cpb.33.4422

Reference yield:

9-acetoxy nonanoic acid (30993-88-5) → Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester (77712-36-8)

Guidance literature:

Multi-step reaction with 4 steps

1: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

2: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

3: 78 percent / NaOH / methanol / 2 h / Ambient temperature

4: H₂, 70percent HClO₄ / 5percent Pd-C / 24 h / Ambient temperature

With sodium hydroxide; aluminium trichloride; perchloric acid; phosphorus pentachloride; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1248/cpb.33.4422

Reference yield:

9-acetoxynonanoyl chloride (30964-05-7) → Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonyl ester (77712-36-8)

Guidance literature:

Multi-step reaction with 3 steps

1: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

2: 78 percent / NaOH / methanol / 2 h / Ambient temperature

3: H₂, 70percent HClO₄ / 5percent Pd-C / 24 h / Ambient temperature

With sodium hydroxide; aluminium trichloride; perchloric acid; hydrogen; palladium on activated charcoal; In methanol; 1,2-dichloro-ethane;

DOI:10.1248/cpb.33.4422

upstream raw materials:

acetic acid

9-Hydroxy-1-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-nonan-1-one

9-acetoxynonal

9-acetoxy nonanoic acid

Downstream raw materials:

2-(9-hydroxynonyl)-5,6-dimethoxy-3-methyl-1,4-benzoquinone

Acetic acid 9-(4,5-dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-nonyl ester

2-(9-Hydroxy-nonyl)-5,6-dimethoxy-3-methyl-phenol