C₃₂H₅₆O₆Si

Base Information

Chemical Name:C₃₂H₅₆O₆Si
CAS No.:1003890-49-0
Molecular Formula:C₃₂H₅₆O₆Si
Molecular Weight:564.879
Hs Code.:

C<sub>32</sub>H<sub>56</sub>O<sub>6</sub>Si

Synonyms:C₃₂H₅₆O₆Si

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Chemical Property of C₃₂H₅₆O₆Si

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Technology Process of C₃₂H₅₆O₆Si

There total 12 articles about C₃₂H₅₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1003890-62-7
1-((4R,6S)-6-((3R,4S,5R)-6-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,5-dimethylhexyl)-2,2-dimethyl-1,3-dioxan-4-yl)-5-methylhex-5-en-2-one

: 1003890-49-0
C₃₂H₅₆O₆Si

Guidance literature:: With cerium(III) chloride; In water; acetonitrile; for 5h;
DOI:10.1021/ol7025944

Reference yield:

: 887143-81-9
(1S,6R,8R)-8-Vinyl-2,9,10-trioxa-1-phospha-bicyclo[4.3.1]dec-4-ene 1-oxide

: 1003890-49-0
C₃₂H₅₆O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: Hoveyda-Grubbs catalyst second generation / 1,1-dichloroethane / 90 °C / Inert atmosphere

2.1: 2-nitrobenzenesulfonyl hydrazide; triethylamine / 1,2-dichloro-ethane / Inert atmosphere

3.1: formic acid; palladium diacetate; triethylamine / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / dichloromethane / Inert atmosphere

6.1: pyridine; ozone / methanol; dichloromethane / -78 °C / Inert atmosphere

6.2: Inert atmosphere

7.1: magnesium / diethyl ether / -78 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / Inert atmosphere

9.1: cerium(III) chloride heptahydrate / water; acetonitrile / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; formic acid; Hoveyda-Grubbs catalyst second generation; cerium(III) chloride heptahydrate; 2-nitrobenzenesulfonyl hydrazide; palladium diacetate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; ozone; magnesium; triethylamine; In methanol; diethyl ether; 1,1-dichloroethane; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jo2003506

Reference yield:

: 887343-98-8
(4R,6R)-2-Allyloxy-4,6-divinyl-[1,3,2]dioxaphosphinane 2-oxide

: 1003890-49-0
C₃₂H₅₆O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane

2.1: Hoveyda-Grubbs catalyst second generation / 1,1-dichloroethane / 90 °C / Inert atmosphere

3.1: 2-nitrobenzenesulfonyl hydrazide; triethylamine / 1,2-dichloro-ethane / Inert atmosphere

4.1: formic acid; palladium diacetate; triethylamine / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

4.2: Inert atmosphere

5.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / dichloromethane / Inert atmosphere

7.1: pyridine; ozone / methanol; dichloromethane / -78 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: magnesium / diethyl ether / -78 °C / Inert atmosphere

9.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / Inert atmosphere

10.1: cerium(III) chloride heptahydrate / water; acetonitrile / Inert atmosphere

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium aluminium tetrahydride; formic acid; Hoveyda-Grubbs catalyst second generation; cerium(III) chloride heptahydrate; 2-nitrobenzenesulfonyl hydrazide; palladium diacetate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; ozone; magnesium; triethylamine; In methanol; diethyl ether; 1,1-dichloroethane; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jo2003506