N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine

Base Information

Chemical Name:N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine
CAS No.:130945-20-9
Molecular Formula:C₄₉H₇₀N₂O₁₀S₄
Molecular Weight:975.366
Hs Code.:

Synonyms:N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine

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Chemical Property of N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine

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Technology Process of N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine

There total 8 articles about N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 130945-16-3
N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

: 104-15-4
toluene-4-sulfonic acid

: 130945-20-9
N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine

Guidance literature:: With N,N'-dimethylaminopyridine; triethylamine; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

: 10160-25-5
7-bromo-1-(2-tetrahydropyranyloxy)heptane

: 130945-20-9
N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg 2.) DMF, 60 deg C, 3 h

2: 99 percent / p-toluenesulfonyl chloride / methanol / 0.5 h / Ambient temperature

3: 92 percent / triethylamine, N,N'-dimethylaminopyridine / CH₂Cl₂ / 2 h / Ambient temperature

With N,N'-dimethylaminopyridine; sodium hydride; triethylamine; p-toluenesulfonyl chloride; In methanol; dichloromethane;

Reference yield:

: 10160-24-4
7-bromoheptyl alcohol

: 130945-20-9
N,N'-di-p-toluenesulfonyl-N,N'-bis<7-(p-toluenesulfonyloxy)heptyl>-1,7-heptanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / p-toluenesulfonic acid / diethyl ether / 14 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg 2.) DMF, 60 deg C, 3 h

3: 99 percent / p-toluenesulfonyl chloride / methanol / 0.5 h / Ambient temperature

4: 92 percent / triethylamine, N,N'-dimethylaminopyridine / CH₂Cl₂ / 2 h / Ambient temperature

With N,N'-dimethylaminopyridine; sodium hydride; toluene-4-sulfonic acid; triethylamine; p-toluenesulfonyl chloride; In methanol; diethyl ether; dichloromethane;