[6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol

Base Information

Chemical Name:[6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol
CAS No.:132113-56-5
Molecular Formula:C₁₉H₂₄O₇
Molecular Weight:364.395
Hs Code.:

Synonyms:[6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol

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Chemical Property of [6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol

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Technology Process of [6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol

There total 4 articles about [6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132113-52-1
3-(2-bromo-3,4,5-trimethoxy-phenyl)-propionic acid

: 132113-56-5
[6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / CH₃COCl / 12 h / 25 °C

2: 72 percent / DIBAL-H / toluene / 0.25 h / -78 °C

3: 93 percent / p-TsOH / benzene / 2 h / Heating

4: 1.) Mg, (CH₂Br)2 / 1.) THF, reflux, 1 h, 2.) reflux, 1.5 h

With diisobutylaluminium hydride; toluene-4-sulfonic acid; magnesium; ethylene dibromide; acetyl chloride; In toluene; benzene;

Reference yield:

: 132113-54-3
3-(2-Bromo-3,4,5-trimethoxy-phenyl)-propionaldehyde

: 132113-56-5
[6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / p-TsOH / benzene / 2 h / Heating

2: 1.) Mg, (CH₂Br)2 / 1.) THF, reflux, 1 h, 2.) reflux, 1.5 h

With toluene-4-sulfonic acid; magnesium; ethylene dibromide; In benzene;

Reference yield:

: 132113-53-2
3-(2-Bromo-3,4,5-trimethoxy-phenyl)-propionic acid methyl ester

: 132113-56-5
[6-(2-[1,3]Dioxolan-2-yl-ethyl)-2,3,4-trimethoxy-phenyl]-furan-2-yl-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / DIBAL-H / toluene / 0.25 h / -78 °C

2: 93 percent / p-TsOH / benzene / 2 h / Heating

3: 1.) Mg, (CH₂Br)2 / 1.) THF, reflux, 1 h, 2.) reflux, 1.5 h

With diisobutylaluminium hydride; toluene-4-sulfonic acid; magnesium; ethylene dibromide; In toluene; benzene;