N-succinimide

Base Information

Chemical Name:N-succinimide
CAS No.:78308-02-8
Molecular Formula:C₁₄H₂₃NO₄
Molecular Weight:269.341
Hs Code.:

N-<rel-(1R,2S,3S)-2,3-bis(2-hydroxyethyl)cyclohexyl>succinimide

Synonyms:N-succinimide

Suppliers and Price of N-succinimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-succinimide

Chemical Property:

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Technology Process of N-succinimide

There total 4 articles about N-succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78308-01-7
N-succinimide

: 78308-02-8
N-succinimide

Guidance literature:: With methanol; sodium tetrahydroborate; ozone; Yield given. Multistep reaction; 1.) -70 deg C, 2.) -70 -> 25 deg C;
DOI:10.1021/jo00330a051

Reference yield:

: 6102-41-6,6102-44-9,14116-78-0,70749-10-9,70749-11-0,78341-47-6
rel-(4aS,8aS)-1,2,3,4,4a,5,8,8a-octahydronaphthalen-2-one

: 78308-02-8
N-succinimide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / lithium aluminum hydride / tetrahydrofuran / 1.) -70 deg C, 75 min, 2.) 3 h

2: 62 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 1.) 0 deg C, 45 min, 2.) room temperature, 30 min

3: 1.) ozone, 2.) sodium borohydride / methanol / 1.) -78 deg C, 43 min

With sodium tetrahydroborate; lithium aluminium tetrahydride; ozone; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol;
DOI:10.1021/ja00343a030

Reference yield:

: 78341-48-7
rel-(1S,4aS,8aS)-1,2,3,4,4a,5,8,8a-ocathydronaphthalen-1-ol

: 78308-02-8
N-succinimide

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 1.) 0 deg C, 45 min, 2.) room temperature, 30 min

2: 1.) ozone, 2.) sodium borohydride / methanol / 1.) -78 deg C, 43 min

With sodium tetrahydroborate; ozone; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol;
DOI:10.1021/ja00343a030