Technology Process of [Pt([5-chloro-2-hydroxyphenylazo]-2-naptholate)(DMSO)]
There total 1 articles about [Pt([5-chloro-2-hydroxyphenylazo]-2-naptholate)(DMSO)] which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
In
dimethyl sulfoxide;
K2(PtCl4) was dissolved in DMSO at 100°C and added to soln. ligand and Na2CO3 in DMSO, heated at 110°C for 1 h; soln. was cooled, water was added, ppt. was filtered, washed with water,MeOH and dried at 100°C, crystn. from toluene at -20°C fo r 12 h; elem. anal.;
DOI:10.1016/j.ica.2006.05.027