2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine

Base Information

• Chemical Name: 2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine
• CAS No.: 1620461-85-9
• Molecular Formula: C₂₆H₃₇N₂P
• Molecular Weight: 408.567
• Mol file: 1620461-85-9.mol

Synonyms:2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine

Chemical Property of 2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine

Chemical Property:

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Technology Process of 2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine

There total 1 articles about 2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2-(bromophenyl)-2'-(dimethylaminophenyl)-amine (1264268-34-9) + chlorodicyclohexylphosphane (16523-54-9) → 2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine (1620461-85-9)

Guidance literature:

2-(bromophenyl)-2'-(dimethylaminophenyl)-amine; With n-butyllithium; In diethyl ether; hexane; at -80 - 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

chlorodicyclohexylphosphane; In diethyl ether; hexane; at -80 - 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c4ob01041h

Reference yield: 86.0%

(1,2-dimethoxyethane)dichloronickel(II) (29046-78-4) + 2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine (1620461-85-9) → C26H36ClN2NiP (1620461-83-7)

Guidance literature:

2-(dicyclohexylphosphinophenyl)-2-(dimethylaminophenyl)amine; With n-butyllithium; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 4h; Inert atmosphere; Schlenk technique;

(1,2-dimethoxyethane)dichloronickel(II); In tetrahydrofuran; hexane; at -80 - 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1039/c4ob01041h

upstream raw materials:

2-(bromophenyl)-2'-(dimethylaminophenyl)-amine

chlorodicyclohexylphosphane

Downstream raw materials:

C₂₆H₃₆ClN₂NiP