3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid

Base Information

Chemical Name:3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid
CAS No.:1053629-07-4
Molecular Formula:C₂₁H₂₄N₆O₇S
Molecular Weight:504.524
Hs Code.:

Synonyms:3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid

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Chemical Property of 3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid

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Technology Process of 3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid

There total 5 articles about 3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26177-44-6
4-bromobenzylamine hydrochloride

: 1053629-07-4
3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / 18-24percent fuming H₂SO₄ / 2 h / 20 - 100 °C

2: 1.) NaOH, 2.) H₂ / 2.) 5percent Pd/C / 1.) water, 2.) water, 50 psi, overnight

3: Et₃N / ethanol / 90 °C

With sodium hydroxide; sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00031a014

Reference yield:

: 152918-55-3
4-bromo-3-sulfobenzylamine

: 1053629-07-4
3-{[9-((3aR,4R,6S,6aS)-2,2-Dimethyl-6-methylcarbamoyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamino]-methyl}-benzenesulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOH, 2.) H₂ / 2.) 5percent Pd/C / 1.) water, 2.) water, 50 psi, overnight

2: Et₃N / ethanol / 90 °C

With sodium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00031a014