methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside
CAS No.:311805-99-9
Molecular Formula:C₃₄H₃₆O₁₄
Molecular Weight:668.651
Hs Code.:

Synonyms:methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Suppliers and Price of methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

There total 6 articles about methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 172364-85-1
methyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: 311805-99-9
methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With acetyl chloride; In methanol; at 20 ℃;
DOI:10.1080/07328300008544122

Reference yield:

: 98-88-4
benzoyl chloride

: 311805-99-9
methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 655 mg / pyridine / 20 °C

2: 90 percent / TMSOTf / CH₂Cl₂ / 1.5 h / -10 - -5 °C

3: 90 percent / acetyl chloride / methanol / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; acetyl chloride; In methanol; dichloromethane; 1: Acylation / 2: Rearrangement / 3: Deacetylation;
DOI:10.1080/07328300008544122

Reference yield:

: 259669-42-6
Acetic acid (2R,3aS,5R,6R,7S,7aS)-6-acetoxy-5-acetoxymethyl-2-methyl-2-((2R,3S,4S,5S,6S)-3,4,5-trihydroxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-[1,3]dioxolo[4,5-b]pyran-7-yl ester

: 311805-99-9
methyl α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 655 mg / pyridine / 20 °C

2: 90 percent / TMSOTf / CH₂Cl₂ / 1.5 h / -10 - -5 °C

3: 90 percent / acetyl chloride / methanol / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; acetyl chloride; In methanol; dichloromethane; 1: Acylation / 2: Rearrangement / 3: Deacetylation;
DOI:10.1080/07328300008544122