C₈H₄⁽²⁾HBr₂NO₂

Base Information

Chemical Name:C₈H₄⁽²⁾HBr₂NO₂
CAS No.:1006060-00-9
Molecular Formula:C₈H₅Br₂NO₂
Molecular Weight:307.933
Hs Code.:

C<sub>8</sub>H<sub>4</sub><sup>(2)</sup>HBr<sub>2</sub>NO<sub>2</sub>

Synonyms:C₈H₄⁽²⁾HBr₂NO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₈H₄⁽²⁾HBr₂NO₂

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Technology Process of C₈H₄⁽²⁾HBr₂NO₂

There total 1 articles about C₈H₄⁽²⁾HBr₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 558-13-4
carbon tetrabromide

: 50344-83-7
2-nitrobenzaldehyde-α-d₁

: 1006060-00-9
C₈H₄⁽²⁾HBr₂NO₂

Guidance literature:: With triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 2.5h;
DOI:10.1021/jo701987r

Reference yield: 23.0%

: 1006060-00-9
C₈H₄⁽²⁾HBr₂NO₂

: 1006059-97-7
2-(2,2-dibromo-1-deuteriovinyl)-phenylamine

Guidance literature:: (E,4S,1'R,2'R,4''R,5''R)-4-(2'-(5''-(dec-1''-en-4''-ynyl)-2'-(4'''-methoxyphenyl)-1',3'-dioxolan-4'-yl)cyclopropyl)-2,2-dimethyl-1,3-dioxolane; With diisobutylaluminium hydride; In dichloromethane; for 53h; cooling;

With tributylphosphine;

With pyridine; dihydrogen peroxide; Further stages.;
DOI:10.1021/jo701739v

Reference yield:

: 1006060-00-9
C₈H₄⁽²⁾HBr₂NO₂

: 1401452-08-1
C₉H₈⁽²⁾HBr₂NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: tin(II) chloride hydrate / ethanol / 0.75 h / Reflux

2: pyridine / dichloromethane / 0 - 20 °C

With pyridine; tin(II) chloride hydrate; In ethanol; dichloromethane;
DOI:10.1039/c2cc34800d