pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone

Base Information

Chemical Name:pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone
CAS No.:1309573-69-0
Molecular Formula:C₁₀H₁₇N₃O₂S
Molecular Weight:243.33
Hs Code.:

pyruvic acid N<sup>(4)</sup>-cyclohexylthiosemicarbazone

Synonyms:pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone

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Chemical Property of pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone

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Technology Process of pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone

There total 1 articles about pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127-17-3
2-oxo-propionic acid

: 21198-18-5
4-cyclohexyl-thiosemicarbazide

: 1309573-69-0,1313191-88-6
pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone

Guidance literature:: In methanol; for 5h; Reflux;
DOI:10.1016/j.jorganchem.2011.09.013

Reference yield: 81.0%

: 1309573-69-0,1313191-88-6
pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone

: 639-58-7
triphenyltin chloride

: (pyruvic acid-N⁽⁴⁾-cyclohexylthiosemicarbazone(-1H))(triphenyltin)

Guidance literature:: In methanol; carbazone dissolved in MeOH in Schlenk flask under N2; then MeOH soln. of Ph3SnCl added dropwise; react. mixt. refluxed for 6 h; cooled to room temp.; ppt. filtered off, washed with cold MeOH; dried in vacuo over silica gel; elem. anal.;
DOI:10.1016/j.poly.2011.11.021

Reference yield: 79.0%

: 1309573-69-0,1313191-88-6
pyruvic acid N⁽⁴⁾-cyclohexylthiosemicarbazone

: 1461-22-9
tributyltin chloride

: (pyruvic acid-N⁽⁴⁾-cyclohexylthiosemicarbazone(-1H))(tributyltin)

Guidance literature:: In methanol; carbazone dissolved in MeOH in Schlenk flask under N2; then MeOH soln. of tBu3SnCl added dropwise; react. mixt. refluxed for 6 h; cooled to roomtemp.; ppt. filtered off, washed with cold MeOH; dried in vacuo over silica gel; elem. anal.;
DOI:10.1016/j.poly.2011.11.021