N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

Base Information

Chemical Name:N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine
CAS No.:255883-46-6
Molecular Formula:C₄₆H₄₂N₄
Molecular Weight:650.866
Hs Code.:

Synonyms:N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

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Technology Process of N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

There total 5 articles about N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 255883-42-2
N,N'-bis(4-bromophenyl)-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

: 106-49-0,12221-03-3
p-toluidine

: 255883-46-6
N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

Guidance literature:: With sodium t-butanolate; palladium diacetate; bis(diphenylphosphinyl)ferrocene; In toluene; at 100 - 110 ℃; for 3h;
DOI:10.1021/ol9912276

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 255883-46-6
N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / t-BuONa / Pd(OAc)2; bis(diphenylphosphinyl)ferrocene / toluene / 24 h / 100 - 110 °C

2: 95 percent / t-BuONa / Pd(OAc)2; bis(diphenylphosphinyl)ferrocene / toluene / 3 h / 100 - 110 °C

With sodium t-butanolate; palladium diacetate; bis(diphenylphosphinyl)ferrocene; In toluene;
DOI:10.1021/ol9912276

Reference yield:

: 108-36-1
1,3-dibromobenzene

: 255883-46-6
N,N'-bis{4-(4-methylanilino)phenyl}-N,N'-bis(4-methylphenyl)-1,3-benzenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / t-BuONa / Pd(OAc)2; bis(diphenylphosphinyl)ferrocene / toluene / 12 h / 100 - 110 °C

2: 73 percent / t-BuONa / Pd(OAc)2; bis(diphenylphosphinyl)ferrocene / toluene / 24 h / 100 - 110 °C

3: 95 percent / t-BuONa / Pd(OAc)2; bis(diphenylphosphinyl)ferrocene / toluene / 3 h / 100 - 110 °C

With sodium t-butanolate; palladium diacetate; bis(diphenylphosphinyl)ferrocene; In toluene;
DOI:10.1021/ol9912276