(R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid

Base Information

Chemical Name:(R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid
CAS No.:1350445-58-7
Molecular Formula:C₄₀H₂₈N₂O₈S
Molecular Weight:696.737
Hs Code.:

Synonyms:(R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid

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Chemical Property of (R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid

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Technology Process of (R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid

There total 3 articles about (R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydro-2-oxa-7-aza-pyren-7-yl)-3-tritylsulfanyl-propionic acid

: 22059-21-8
aminocyclopropane-1-carboxylic acid

: 1350445-58-7
(R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 140 ℃; for 0.0833333h; Sonication; Microwave irradiation;
DOI:10.1039/c1ob06147j

Reference yield:

: 2799-07-7
S-trityl-L-cysteine

: 1350445-58-7
(R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 0.08 h / 40 °C / Microwave irradiation

2: triethylamine / N,N-dimethyl-formamide / 0.08 h / 140 °C / Sonication; Microwave irradiation

With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1039/c1ob06147j

Reference yield:

: 81-30-1
1,4,5,8-naphthalenetetracarboxylic dianhydride

: 1350445-58-7
(R)-1-(7-(1-carboxy-2-(tritylthio)ethyl)-1,3,6,8-tetraoxo-7,8-dihydrobenzo[lmn][3,8]phenanthrolin-2(1H,3H,6H)-yl)cyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 0.08 h / 40 °C / Microwave irradiation

2: triethylamine / N,N-dimethyl-formamide / 0.08 h / 140 °C / Sonication; Microwave irradiation

With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1039/c1ob06147j