2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester

Base Information

Chemical Name:2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester
CAS No.:162404-50-4
Molecular Formula:C₂₈H₂₆O₈
Molecular Weight:490.51
Hs Code.:

Synonyms:2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester

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Chemical Property of 2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester

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Technology Process of 2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester

There total 1 articles about 2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 97729-12-9
methyl 2-[(trimethylsilyl)methyl]benzoate

: 2-[1-Benzo[1,3]dioxol-5-yl-meth-(Z)-ylidene]-malonic acid benzyl ester methyl ester

: 162404-50-4
2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester

Guidance literature:: With cesium fluoride; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 60 ℃; for 3h;
DOI:10.1016/S0968-0896(98)00022-4

Reference yield:

: 162404-50-4
2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester

: 2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid monomethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 7h; Ambient temperature;
DOI:10.1016/S0968-0896(98)00022-4

Reference yield:

: 162404-50-4
2-[1-Benzo[1,3]dioxol-5-yl-2-(2-methoxycarbonyl-phenyl)-ethyl]-malonic acid benzyl ester methyl ester

: 162404-52-6
2-(2-Benzo[1,3]dioxol-5-yl-3-methoxycarbonyl-propyl)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate / 7 h / Ambient temperature

2: 1 h / 150 °C

With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0968-0896(98)00022-4