Technology Process of N-phenyl-N-[2-(9-methyl)carbazolyl]amine
There total 5 articles about N-phenyl-N-[2-(9-methyl)carbazolyl]amine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate;
In
o-xylene;
at 130 ℃;
for 8h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water; dimethyl sulfoxide / 2 h / 70 °C / Inert atmosphere
2: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 8 h / 130 °C / Inert atmosphere
With
N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate;
In
o-xylene; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 8 h / Inert atmosphere; Reflux
2: triethyl phosphite / nitrogen / 24 h / 150 °C / Inert atmosphere
3: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water; dimethyl sulfoxide / 2 h / 70 °C / Inert atmosphere
4: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 8 h / 130 °C / Inert atmosphere
With
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; sodium hydroxide; sodium t-butanolate; triethyl phosphite;
tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine; palladium diacetate;
In
tetrahydrofuran; o-xylene; nitrogen; water; dimethyl sulfoxide;
