4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline

Base Information

Chemical Name:4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline
CAS No.:1310371-04-0
Molecular Formula:C₃₉H₂₉N₃OS
Molecular Weight:587.745
Hs Code.:

Synonyms:4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline

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Chemical Property of 4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline

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Technology Process of 4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline

There total 1 articles about 4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.2%

: 267221-88-5
4-(diphenylamino)phenylboronic pinacol ester

: 1310371-00-6
4-(5-bromothiophen-2-yl)-6-(3-methoxyphenyl)-2,2'-bipyridine

: 1310371-04-0
4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 65 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ic1025679

Reference yield: 55.2%

: 330680-47-2
trichloro(trimethyl-4,4',4''-tricarboxylate-2,2':6',2''-terpyridine)ruthenium

: 1310371-04-0
4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline

: 7732-18-5
water

: silver nitrate

: (4-[5-[6-(3-methoxyphenyl)-2,2'-bipyridin-4-yl]thiophen-2-yl]-N,N-diphenylaniline(-1H))(trimethyl-4,4',4''-tricarboxylate-2,2':6',2''-terpyridine)ruthenium(II) nitrate dihydrate

Guidance literature:: With N-ethylmorpholine; In tetrahydrofuran; methanol; water; Ru complex and N-ethylmorpholine added to MeOH-H2O-THF soln. of ligand; refluxed for 16 h; AgNO3 added; refluxed for 1.5 h; cooled; preabsorbed on silica; solvent removed in vac.; purified by column chromy. (silica, CH2Cl2-MeOH 9:1); elem. anal.;
DOI:10.1021/ic1025679