C₁₉H₁₃FN₂O

Base Information

Chemical Name:C₁₉H₁₃FN₂O
CAS No.:1367127-15-8
Molecular Formula:C₁₉H₁₃FN₂O
Molecular Weight:304.323
Hs Code.:

C<sub>19</sub>H<sub>13</sub>FN<sub>2</sub>O

Synonyms:C₁₉H₁₃FN₂O

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Chemical Property of C₁₉H₁₃FN₂O

Chemical Property:

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Technology Process of C₁₉H₁₃FN₂O

There total 8 articles about C₁₉H₁₃FN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1367127-13-6
C₁₉H₁₅FN₂O₂

: 1367127-15-8
C₁₉H₁₃FN₂O

Guidance literature:: With triethylamine; trifluoroacetic anhydride; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 371-41-5
4-Fluorophenol

: 1367127-15-8
C₁₉H₁₃FN₂O

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 120 °C

2.1: hydrogen / 5%-palladium/activated carbon / methanol / 20 °C / Inert atmosphere

3.1: sulfuric acid / 1,2-dimethoxyethane; water

3.2: 0.83 h / 0 - 5 °C

3.3: 0.5 h / 0 °C

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 0.17 h / 20 °C / Inert atmosphere

4.2: 18 h / 90 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / tetrahydrofuran / 3 h / 75 °C

6.1: ammonia / methanol / 12 h / 20 °C

7.1: triethylamine; trifluoroacetic anhydride / dichloromethane / 1 h / 0 °C

With sulfuric acid; tetrabutyl ammonium fluoride; ammonia; hydrogen; potassium carbonate; triethylamine; trifluoroacetic anhydride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; 5%-palladium/activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1367127-15-8
C₁₉H₁₃FN₂O

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 120 °C

2.1: hydrogen / 5%-palladium/activated carbon / methanol / 20 °C / Inert atmosphere

3.1: sulfuric acid / 1,2-dimethoxyethane; water

3.2: 0.83 h / 0 - 5 °C

3.3: 0.5 h / 0 °C

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 0.17 h / 20 °C / Inert atmosphere

4.2: 18 h / 90 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / tetrahydrofuran / 3 h / 75 °C

6.1: ammonia / methanol / 12 h / 20 °C

7.1: triethylamine; trifluoroacetic anhydride / dichloromethane / 1 h / 0 °C

With sulfuric acid; tetrabutyl ammonium fluoride; ammonia; hydrogen; potassium carbonate; triethylamine; trifluoroacetic anhydride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; 5%-palladium/activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;