t-butyl triphenylsilyl(phenylmethyl)carbamate

Base Information

Chemical Name:t-butyl triphenylsilyl(phenylmethyl)carbamate
CAS No.:548780-42-3
Molecular Formula:C₃₀H₃₁NO₂Si
Molecular Weight:465.667
Hs Code.:

Synonyms:t-butyl triphenylsilyl(phenylmethyl)carbamate

Suppliers and Price of t-butyl triphenylsilyl(phenylmethyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of t-butyl triphenylsilyl(phenylmethyl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of t-butyl triphenylsilyl(phenylmethyl)carbamate

There total 1 articles about t-butyl triphenylsilyl(phenylmethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 42116-44-9
N-tert-butoxycarbonylbenzylamine

: 18752-21-1
allyltriphenylsilane

: 548780-42-3
t-butyl triphenylsilyl(phenylmethyl)carbamate

Guidance literature:: allyltriphenylsilane; With trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 1h;

N-tert-butoxycarbonylbenzylamine; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/ol034397y

Reference yield: 80.0%

: 548780-42-3
t-butyl triphenylsilyl(phenylmethyl)carbamate

: 548780-40-1
tert-butyl [(triphenylsilanyl)phenylmethyl]carbamate

Guidance literature:: With sec.-butyllithium; In cyclohexane; toluene; at -78 - -20 ℃; for 2h;
DOI:10.1021/ol034397y

Reference yield:

: 548780-42-3
t-butyl triphenylsilyl(phenylmethyl)carbamate

: α-[(triphenylsilanyl)-phenylmethyl]amine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / sec-butyllithium / toluene; cyclohexane / 2 h / -78 - -20 °C

2: 96 percent / sodium iodide; chlorotrimethylsilane; triethylamine / acetonitrile / 0.5 h

With chloro-trimethyl-silane; sec.-butyllithium; triethylamine; sodium iodide; In cyclohexane; toluene; acetonitrile; 1: reverse aza-Brook rearrangement;
DOI:10.1021/ol034397y