2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide

Base Information

Chemical Name:2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide
CAS No.:402921-65-7
Molecular Formula:C₃₃H₃₅N₅O₃
Molecular Weight:549.673
Hs Code.:

Synonyms:2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide

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Chemical Property of 2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide

Chemical Property:

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Technology Process of 2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide

There total 9 articles about 2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 86506-70-9
rac-2-(2-(oxiran-2-yl)ethyl)isoindoline-1,3-dione

: 402921-64-6
N-benzyl-N’,N’-bis(2-pyridylmethyl)-1,2-diaminoethane

: 402921-65-7
2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide

Guidance literature:: In butan-1-ol; at 100 ℃; for 8h;
DOI:10.1039/b103164n

Reference yield:

: 189440-33-3
(2-aminoethyl)bis(2-pyridylmethyl)amine

: 402921-65-7
2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

2: 91 percent / NaBH₄ / acetonitrile; acetic acid; ethanol / 18 h / 20 °C

3: 82 percent / butan-1-ol / 8 h / 100 °C

With sodium tetrahydroborate; magnesium sulfate; In ethanol; dichloromethane; acetic acid; acetonitrile; butan-1-ol;
DOI:10.1039/b103164n

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 402921-65-7
2-(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-3-hydroxybutyl)phthalimide

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

2: 73 percent / NaBH₄ / acetonitrile; ethanol; acetic acid / 18 h / 20 °C

3: 68 percent / K₂CO₃; KI / acetonitrile / 24 h / Heating

4: 68 percent / hydrazine monohydrate / ethanol / 3 h / Heating

5: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

6: 91 percent / NaBH₄ / acetonitrile; acetic acid; ethanol / 18 h / 20 °C

7: 82 percent / butan-1-ol / 8 h / 100 °C

With sodium tetrahydroborate; magnesium sulfate; potassium carbonate; hydrazine hydrate; potassium iodide; In ethanol; dichloromethane; acetic acid; acetonitrile; butan-1-ol;
DOI:10.1039/b103164n