methyl 3-(acetylamino)-4-O-benzoyl-6-bromo-2,3,6-trideoxyhexopyranoside

Base Information

Chemical Name:methyl 3-(acetylamino)-4-O-benzoyl-6-bromo-2,3,6-trideoxyhexopyranoside
CAS No.:63554-16-5
Molecular Formula:C16H20 Br N O5
Molecular Weight:386.2377
Hs Code.:

Synonyms:NSC276416

Suppliers and Price of methyl 3-(acetylamino)-4-O-benzoyl-6-bromo-2,3,6-trideoxyhexopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of methyl 3-(acetylamino)-4-O-benzoyl-6-bromo-2,3,6-trideoxyhexopyranoside

Chemical Property:

Boiling Point:540.4°Cat760mmHg
Flash Point:280.6°C
Density:1.42g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 3-(acetylamino)-4-O-benzoyl-6-bromo-2,3,6-trideoxyhexopyranoside

There total 6 articles about methyl 3-(acetylamino)-4-O-benzoyl-6-bromo-2,3,6-trideoxyhexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.9%

: 63598-34-5
Methyl 3-acetamido-4,6-O-benzylidene-2,3-dideoxy-α-D-arabino-hexopyranoside

: 63554-16-5
Methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 6h; Heating;
DOI:10.1055/s-2000-6328

Reference yield:

: 63598-31-2
methyl 4,6-O-(R)-benzylidene-2-deoxy-α-D-erythrohexopyranosid-3-ulose

: 63554-16-5
Methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: NaBH₄ / methanol / 2 h / 0 - 20 °C

2: pyridine / CH₂Cl₂ / 0.75 h / 20 °C

3: NaN₃ / dimethylformamide / 1.5 h / 20 °C

4: LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

5: pyridine / 2 h / 20 °C

6: 75.9 percent / NBS; BaCO₃ / CCl₄ / 6 h / Heating

With pyridine; sodium tetrahydroborate; N-Bromosuccinimide; lithium aluminium tetrahydride; sodium azide; barium carbonate; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; 1: Reduction / 2: Esterification / 3: Substitution / 4: Reduction / 5: Acetylation / 6: Substitution;
DOI:10.1055/s-2000-6328

Reference yield:

: 102916-74-5
Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-α-D-arabino-hexopyranoside

: 63554-16-5
Methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

2: pyridine / 2 h / 20 °C

3: 75.9 percent / NBS; BaCO₃ / CCl₄ / 6 h / Heating

With pyridine; N-Bromosuccinimide; lithium aluminium tetrahydride; barium carbonate; In tetrahydrofuran; tetrachloromethane; 1: Reduction / 2: Acetylation / 3: Substitution;
DOI:10.1055/s-2000-6328