C₃₂H₃₄FNO₇S

Base Information

Chemical Name:C₃₂H₃₄FNO₇S
CAS No.:1374234-42-0
Molecular Formula:C₃₂H₃₄FNO₇S
Molecular Weight:595.689
Hs Code.:

C<sub>32</sub>H<sub>34</sub>FNO<sub>7</sub>S

Synonyms:C₃₂H₃₄FNO₇S

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Chemical Property of C₃₂H₃₄FNO₇S

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Technology Process of C₃₂H₃₄FNO₇S

There total 8 articles about C₃₂H₃₄FNO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1374234-41-9
C₂₇H₂₆FNO₇S

: 1119-51-3
bromopentene

: 1374234-42-0
C₃₂H₃₄FNO₇S

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374234-42-0
C₃₂H₃₄FNO₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

7.1: pyridine / dichloromethane / 3 h / 0 °C

8.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

With pyridine; potassium phosphate; hydrogen; nitric acid; sodium hydride; potassium carbonate; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374234-42-0
C₃₂H₃₄FNO₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

6.1: pyridine / dichloromethane / 3 h / 0 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

With pyridine; potassium phosphate; hydrogen; nitric acid; potassium carbonate; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;