4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide
CAS No.:102607-79-4
Molecular Formula:C₁₅H₁₃F₃N₂O₃S
Molecular Weight:358.341
Hs Code.:

Synonyms:4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide

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Chemical Property of 4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide

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Technology Process of 4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide

There total 3 articles about 4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 102607-79-4
4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide

Guidance literature:: With palladium diacetate; In acetonitrile; at 20 ℃; for 12h; under 20 Torr;

Reference yield: 87.0%

: 455-14-1
4-trifluoromethylphenylamine

: 4083-64-1
Tosyl isocyanate

: 102607-79-4
4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide

Guidance literature:: In dichloromethane;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 102607-79-4
4-methyl-N-[[(4-trifluoromethylphenyl)amino]carbonyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / water; acetonitrile / 0.33 h / 20 °C / Schlenk technique

2: palladium diacetate / acetonitrile / 20 °C / 15 Torr / Schlenk technique; Sealed tube

With sodium azide; palladium diacetate; In water; acetonitrile;
DOI:10.1002/anie.201600887