(+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate

Base Information

Chemical Name:(+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate
CAS No.:1309655-38-6
Molecular Formula:C₁₂H₂₃F₂NO₂Si
Molecular Weight:279.402
Hs Code.:

Synonyms:(+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate

Suppliers and Price of (+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate

There total 2 articles about (+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₉F₂NO₃Si

: 1309655-38-6
(+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201100113

Reference yield:

: 911395-49-8
2-(trimethylsilyl)ethyl 6,6-difluoro-1-[(4-methoxyphenyl)amino]-3-cyclohexene-1-carboxylate

: 1309655-38-6
(+/-)-2-(trimethylsilyl)ethyl 1-amino-2,2-difluorocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 7757.43 Torr / Inert atmosphere

2: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 0 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; palladium 10% on activated carbon; hydrogen; In water; ethyl acetate; acetonitrile;
DOI:10.1002/chem.201100113