C₁₃H₁₆O

Base Information

Chemical Name:C₁₃H₁₆O
CAS No.:1429412-53-2
Molecular Formula:C₁₃H₁₆O
Molecular Weight:188.269
Hs Code.:

Synonyms:C₁₃H₁₆O

Suppliers and Price of C₁₃H₁₆O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₆O

Chemical Property:

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Technology Process of C₁₃H₁₆O

There total 12 articles about C₁₃H₁₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1429412-56-5
C₆H₁₀O

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 1429412-53-2
C₁₃H₁₆O

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; at 0 ℃; for 16h;
DOI:10.1039/c3ob27508f

Reference yield:

: 90965-06-3
dimethyl 1-(1-diazo-2-oxopropyl)phosphonate

: 126394-25-0
(S)-2-(benzyloxymethyl)butanal

: 1429412-53-2
C₁₃H₁₆O

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 8h;
DOI:10.1039/c3ob27508f

Reference yield:

: 133-13-1
ethyl diethyl malonate

: 1429412-53-2
C₁₃H₁₆O

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16.5 h / -10 - 20 °C

2.1: sodium hydride / nujol; tetrahydrofuran / 16.5 h / 0 - 20 °C

2.2: 3 h / 0 - 20 °C

3.1: Amano lipase / di-isopropyl ether / 12 h / 20 °C / Enzymatic reaction

4.1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 16 h / 0 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

6.2: -78 - 20 °C

7.1: potassium carbonate / methanol / 8 h / 20 °C

With lithium aluminium tetrahydride; oxalyl dichloride; trifluorormethanesulfonic acid; Amano lipase; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; dimethyl sulfoxide; In tetrahydrofuran; methanol; nujol; dichloromethane; di-isopropyl ether; cyclohexane; 6.1: |Swern Oxidation / 6.2: |Swern Oxidation;
DOI:10.1039/c3ob27508f