1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide

Base Information

Chemical Name:1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide
CAS No.:1598427-89-4
Molecular Formula:C₁₉H₂₀N₄O₅
Molecular Weight:384.392
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide

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Chemical Property of 1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide

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Technology Process of 1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide

There total 4 articles about 1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.9%

: 893777-38-3
4-[(4-methoxyphenyl)hydrazono]-2-(3,4,5-trimethoxyphenyl)-4H-oxazol-5-one

: 1598427-89-4
1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide

Guidance literature:: With ammonium hydroxide; In methanol; water; for 0.5h; Reflux;
DOI:10.1016/j.ejmech.2014.03.001

Reference yield:

: 36974-48-8
2-(3,4,5-trimethoxy-phenyl)-4H-oxazol-5-one

: 1598427-89-4
1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0.17 h / -5 - 0 °C

1.2: 2 h / 0 - 10 °C

2.1: ammonium hydroxide / water; methanol / 0.5 h / Reflux

With hydrogenchloride; ammonium hydroxide; sodium nitrite; In methanol; water;
DOI:10.1016/j.ejmech.2014.03.001

Reference yield:

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 1598427-89-4
1-(4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1H-[1,2,4]triazole-3-carboxylic acid amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide

2.1: acetic anhydride / Heating

3.1: sodium nitrite; hydrogenchloride / water / 0.17 h / -5 - 0 °C

3.2: 2 h / 0 - 10 °C

4.1: ammonium hydroxide / water; methanol / 0.5 h / Reflux

With hydrogenchloride; ammonium hydroxide; acetic anhydride; sodium hydroxide; sodium nitrite; In methanol; water;
DOI:10.1016/j.ejmech.2014.03.001