17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

Base Information

Chemical Name:17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane
CAS No.:284666-53-1
Molecular Formula:C₄₀H₅₅N₃O₇
Molecular Weight:689.893
Hs Code.:

Synonyms:17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

Suppliers and Price of 17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

There total 10 articles about 17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 129245-21-2
O-benzyl-N-(5-aminopentyl)-N-(tert-butoxycarbonyl)hydroxylamine

: 284666-50-8
N-(benzyloxy)-N-(5-benzyloxypentyl)succinamic acid

: 284666-53-1
17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

Guidance literature:: With diphenyl-phosphinic acid; triethylamine; In acetonitrile; at 0 - 20 ℃;
DOI:10.1021/jo000050m

Reference yield:

: 6280-87-1
δ-chlorovaleronitrile

: 284666-53-1
17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaH; NaI / dimethylformamide

2: 91 percent / H₂; NH₃ / Raney Ni / methanol

3: 91 percent / DPPA; Et₃N / acetonitrile / 0 - 20 °C

With diphenyl-phosphinic acid; ammonia; hydrogen; sodium hydride; triethylamine; sodium iodide; nickel; In methanol; N,N-dimethyl-formamide; acetonitrile; 1: Substitution / 2: Catalytic hydrogenation / 3: Acylation;
DOI:10.1021/jo000050m

Reference yield:

: 79722-21-7
tert-butyl N-(benzyloxy)carbamate

: 284666-53-1
17-(tert-butoxycarbonyl)-1,6,17-tris(benzyloxy)-7,10-dioxo-6,11,17-triazaheptadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaH; NaI / dimethylformamide

2: 91 percent / H₂; NH₃ / Raney Ni / methanol

3: 91 percent / DPPA; Et₃N / acetonitrile / 0 - 20 °C

With diphenyl-phosphinic acid; ammonia; hydrogen; sodium hydride; triethylamine; sodium iodide; nickel; In methanol; N,N-dimethyl-formamide; acetonitrile; 1: Substitution / 2: Catalytic hydrogenation / 3: Acylation;
DOI:10.1021/jo000050m