succinimido 3-azido-5-(azidomethyl)benzoate

Base Information

Chemical Name:succinimido 3-azido-5-(azidomethyl)benzoate
CAS No.:1620809-47-3
Molecular Formula:C₁₂H₉N₇O₄
Molecular Weight:315.248
Hs Code.:

Synonyms:succinimido 3-azido-5-(azidomethyl)benzoate

Suppliers and Price of succinimido 3-azido-5-(azidomethyl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of succinimido 3-azido-5-(azidomethyl)benzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of succinimido 3-azido-5-(azidomethyl)benzoate

There total 6 articles about succinimido 3-azido-5-(azidomethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.1%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 1310822-77-5
3-azido-5-(azidomethyl)-benzoic acid

: 1620809-47-3
succinimido 3-azido-5-(azidomethyl)benzoate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 22h; Inert atmosphere;
DOI:10.1002/ejoc.201402516

Reference yield:

: 99-36-5
1-methoxycarbonyl-3-methylbenzene

: 1620809-47-3
succinimido 3-azido-5-(azidomethyl)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / hexane / 20 °C / Inert atmosphere

2: trimethylsilylazide; copper(l) chloride; potassium fluoride / methanol / 20 - 70 °C

3: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3 h / 20 - 90 °C / Inert atmosphere

4: sodium azide / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

5: sodium hydroxide / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 22 h / 0 - 20 °C / Inert atmosphere

With potassium fluoride; N-Bromosuccinimide; sodium azide; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 2,2'-azobis(isobutyronitrile); trimethylsilylazide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 4,4'-di-tert-butyl-2,2'-bipyridine; copper(l) chloride; sodium hydroxide; In tetrahydrofuran; methanol; tetrachloromethane; hexane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201402516

Reference yield:

: 1620809-36-0
methyl 3-azido-5-methylbenzoate

: 1620809-47-3
succinimido 3-azido-5-(azidomethyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3 h / 20 - 90 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

3: sodium hydroxide / methanol; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 22 h / 0 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; sodium azide; 2,2'-azobis(isobutyronitrile); 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201402516