C₉⁽¹³⁾CH₁₃NO

Base Information

Chemical Name:C₉⁽¹³⁾CH₁₃NO
CAS No.:264279-40-5
Molecular Formula:C₁₀H₁₃NO
Molecular Weight:164.208
Hs Code.:

C<sub>9</sub><sup>(13)</sup>CH<sub>13</sub>NO

Synonyms:C₉⁽¹³⁾CH₁₃NO

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Chemical Property of C₉⁽¹³⁾CH₁₃NO

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Technology Process of C₉⁽¹³⁾CH₁₃NO

There total 6 articles about C₉⁽¹³⁾CH₁₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 264279-39-2
C₉⁽¹³⁾CH₁₅NO

: 264279-40-5
C₉⁽¹³⁾CH₁₃NO

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/(SICI)1099-0690(200003)2000:5<829::AID-EJOC829>3.0.CO;2-Z

Reference yield:

: 125095-55-8
[2-13C]-5-methyl-4-hexenenitrile

: 264279-40-5
C₉⁽¹³⁾CH₁₃NO

Guidance literature:: Multi-step reaction with 6 steps

1.1: 82 percent / diethyl ether / 1 h / 0 °C

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 51 percent / tetrahydrofuran / 2 h / 20 °C

3.1: 91 percent / conc. H₂SO₄ / nitromethane / 0.5 h / 0 °C

4.1: 80 percent / m-chloroperbenzoic acid / ethyl acetate / 0 - 20 °C

5.1: 1.92 g / LDA / tetrahydrofuran / -40 - 20 °C

6.1: 60 percent / pyridinium chlorochromate / CH₂Cl₂ / 0 - 20 °C

With sulfuric acid; sodium hydride; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; nitromethane; dichloromethane; ethyl acetate; 1.1: Methylation / 2.1: Metallation / 2.2: Condensation / 3.1: Cyclization / 4.1: Epoxidation / 5.1: Isomerization / 6.1: Oxidation;
DOI:10.1002/(SICI)1099-0690(200003)2000:5<829::AID-EJOC829>3.0.CO;2-Z

Reference yield:

: C₇⁽¹³⁾CH₁₄O

: 264279-40-5
C₉⁽¹³⁾CH₁₃NO

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / tetrahydrofuran / 0 - 20 °C

1.2: 51 percent / tetrahydrofuran / 2 h / 20 °C

2.1: 91 percent / conc. H₂SO₄ / nitromethane / 0.5 h / 0 °C

3.1: 80 percent / m-chloroperbenzoic acid / ethyl acetate / 0 - 20 °C

4.1: 1.92 g / LDA / tetrahydrofuran / -40 - 20 °C

5.1: 60 percent / pyridinium chlorochromate / CH₂Cl₂ / 0 - 20 °C

With sulfuric acid; sodium hydride; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; nitromethane; dichloromethane; ethyl acetate; 1.1: Metallation / 1.2: Condensation / 2.1: Cyclization / 3.1: Epoxidation / 4.1: Isomerization / 5.1: Oxidation;
DOI:10.1002/(SICI)1099-0690(200003)2000:5<829::AID-EJOC829>3.0.CO;2-Z