2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide

Base Information

Chemical Name:2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide
CAS No.:119805-76-4
Molecular Formula:C₂₃H₂₅N₇O
Molecular Weight:415.498
Hs Code.:

Synonyms:2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide

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Chemical Property of 2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide

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Technology Process of 2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide

There total 3 articles about 2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119805-70-8
{1-[2-(6-Dimethylamino-purin-9-ylmethyl)-phenylcarbamoyl]-2-phenyl-ethyl}-carbamic acid benzyl ester

: 119805-76-4
2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; acetic acid; under 1520 - 2280 Torr;
DOI:10.1016/0223-5234(88)90202-4

Reference yield:

: 10549-98-1
dimethyl-[9-(2-nitro-benzyl)-9H-purin-6-yl]-amine

: 119805-76-4
2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂ / 10percent Pd/C / acetic acid / 1.5 h / 1520 - 2280 Torr

2: 1.) triethylamine, ethyl chloroformate / 1.) THF, 10 min; 2.) THF, acetic acid, r.t., 15 h

3: H₂ / 10percent Pd/C / acetic acid; methanol / 1520 - 2280 Torr

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1016/0223-5234(88)90202-4

Reference yield:

: 112089-26-6
6-(Dimethylamino)-9-(2-aminobenzyl)-9H-purine

: 119805-76-4
2-Amino-N-[2-(6-dimethylamino-purin-9-ylmethyl)-phenyl]-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triethylamine, ethyl chloroformate / 1.) THF, 10 min; 2.) THF, acetic acid, r.t., 15 h

2: H₂ / 10percent Pd/C / acetic acid; methanol / 1520 - 2280 Torr

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1016/0223-5234(88)90202-4