Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid

Base Information

Chemical Name:Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid
CAS No.:113035-36-2
Molecular Formula:C₂₉H₃₇Cl₂N₃O₆
Molecular Weight:594.535
Hs Code.:

Synonyms:Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid

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Chemical Property of Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid

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Technology Process of Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid

There total 4 articles about Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2483-46-7
Boc-Lys(Boc)-OH

: 113055-87-1
2,6-Dichlor-N-phenylbenzimidchlorid

: 113035-36-2
Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid

Guidance literature:: With triethylamine; In acetone; for 4h; Ambient temperature;

Reference yield:

: 3797-94-2
2,6-dichloro-N-phenylbenzamide

: 113035-36-2
Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / PCl₅ / 1 h / Heating

2: 99 percent / NEt₃ / acetone / 4 h / Ambient temperature

With phosphorus pentachloride; triethylamine; In acetone;

Reference yield:

: 62-53-3
aniline

: 113035-36-2
Nα,Nε-Bis(tert-butoxycarbonyl)-N-(2,6-dichlorbenzoyl)-N-phenyl-L-lysinamid

Guidance literature:: Multi-step reaction with 3 steps

2: 86 percent / PCl₅ / 1 h / Heating

3: 99 percent / NEt₃ / acetone / 4 h / Ambient temperature

With phosphorus pentachloride; triethylamine; In acetone;