[(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)]

Base Information

Chemical Name:[(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)]
CAS No.:1195984-83-8
Molecular Formula:C₅₈H₅₀Ni₂P₄S₄
Molecular Weight:1116.57
Hs Code.:

Synonyms:[(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)]

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Chemical Property of [(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)]

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Technology Process of [(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)]

There total 2 articles about [(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108970-88-3
benzo[1,2-d:4,5-d′]bis([1,3]dithiole)-2,6-dione

: 1195984-83-8
[(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)]

Guidance literature:: With LiOCH₃; In tetrahydrofuran; methanol; (N2); stirring mixt. of s-indacene deriv., dry 1:1 THF/methanol and methanolic soln. of lithium methylate for 1 h, addn. of 1,2-bis(diphenylphosphino)ethanenickel(II) dihalide, stirring for 12 h at room temp.; filtration, washing with diethyl ether, elem. anal.;
DOI:10.1021/ic901257s

Reference yield: 81.0%

: 14647-23-5
1,2-bis(diphenylphosphino)ethane nickel(II) chloride

: 1007121-94-9
(1,2,4,5-benzenetetrathiolato)bis(dibutyltin)

: 1195984-83-8
[(Ni(1,2-bis(diphenylphosphino)ethane))2(1,2,4,5-benzenetetrathiolate)]

Guidance literature:: In further solvent(s); (N2); refluxing mixt. of nickel compd., tin compd. and ClCH2CH2Cl for 12h; filtration, washing with methanol and diethyl ether, drying in vac., elem. anal.;
DOI:10.1021/ic901257s