tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate

Base Information

Chemical Name:tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate
CAS No.:521964-59-0
Molecular Formula:C₁₅H₂₅NO₄
Molecular Weight:283.368
Hs Code.:2924299090
DSSTox Substance ID:DTXSID20584918
Nikkaji Number:J2.140.829H
Mol file:521964-59-0.mol

Synonyms:521964-59-0;tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate;tert-butyl 1-[(2-methylpropan-2-yl)oxycarbonylamino]cyclopent-3-ene-1-carboxylate;1-[[(1,1-Dimethylethoxy)carbonyl]amino]-3-cyclopentene-1-carboxylic acid 1,1-dimethylethyl ester;SCHEMBL1088061;DTXSID20584918;CDPAAIMSAXXWQH-UHFFFAOYSA-N;tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate, 97%;1-(tert-butoxycarbonylamino)-1-(tert-butoxycarbonyl)cyclopent-3-ene;TERT-BUTYL 1-[(TERT-BUTOXYCARBONYL)AMINO]CYCLOPENT-3-ENE-1-CARBOXYLATE;3-Cyclopentene-1-carboxylicacid,1-[[(1,1-dimethylethoxy)carbonyl]amino]-,1,1-dimethylethyl ester

Suppliers and Price of tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate 97%
500mg
$ 124.00

American Custom Chemicals Corporation
tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate 95.00%
500MG
$ 680.96

Total 5 raw suppliers

Chemical Property of tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:86-90 °C
Boiling Point:362.26°C at 760 mmHg
Flash Point:172.889°C
PSA：64.63000
Density:1.066g/cm³
LogP:3.33250
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:283.17835828
Heavy Atom Count:20
Complexity:405

Purity/Quality:

98%Min ^*data from raw suppliers

tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)C1(CC=CC1)NC(=O)OC(C)(C)C

Technology Process of tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate

There total 8 articles about tert-Butyl 1-(Boc-amino)-3-cyclopentene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 75-65-0
tert-butyl alcohol

: 635318-61-5
3-cyclopentene-1,1-dicarboxylic acid mono(1,1-dimethylethyl) ester

: 521964-59-0
tert-butyl 1-tert-butoxycarbonylaminocyclopent-3-enecarboxylate

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; at 85 ℃; for 10h;
DOI:10.1055/s-2004-831218

Reference yield:

: 635318-64-8
1-(isocyanate)-1-(tert-butoxycarbonyl)cyclopent-3-ene

: 75-65-0
tert-butyl alcohol

: 521964-59-0
tert-butyl 1-tert-butoxycarbonylaminocyclopent-3-enecarboxylate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; toluene; at 0 - 23 ℃; for 3h;

Reference yield:

: 635318-64-8
1-(isocyanate)-1-(tert-butoxycarbonyl)cyclopent-3-ene

: 865-47-4
potassium tert-butylate

: 521964-59-0
tert-butyl 1-tert-butoxycarbonylaminocyclopent-3-enecarboxylate

Guidance literature:: 1-(isocyanate)-1-(tert-butoxycarbonyl)cyclopent-3-ene; potassium tert-butylate; In toluene; tert-butyl alcohol; at 0 - 23 ℃; for 1.66667h; Large scale;

With water; In tert-butyl methyl ether; toluene; tert-butyl alcohol; at 20 - 30 ℃; Large scale;
DOI:10.1021/op060225f