(6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol

Base Information

Chemical Name:(6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol
CAS No.:335455-27-1
Molecular Formula:C₂₈H₄₀O₂Si
Molecular Weight:436.71
Hs Code.:

Synonyms:(6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol

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Chemical Property of (6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol

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Technology Process of (6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol

There total 5 articles about (6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 335455-26-0
C₃₄H₅₄O₂Si₂

: 335455-27-1
(6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol

Guidance literature:: pyridinium p-toluenesulfonate; In ethanol; at 23 ℃; for 6h;
DOI:10.1021/ol015667k

Reference yield:

: 335455-23-7
(E)-7-iodo-6-methylhept-6-en-1-ol

: 335455-27-1
(6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 90 percent / imidazole; DMAP / dimethylformamide

2.1: n-BuLi / diethyl ether / -78 °C

2.2: diethyl ether / -78 - 0 °C

3.1: 86 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

4.1: 87 percent / PPTS / ethanol / 6 h / 23 °C

With 1H-imidazole; dmap; n-butyllithium; potassium hexamethylsilazane; pyridinium p-toluenesulfonate; In tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ol015667k

Reference yield:

: 335455-24-8
tert-butyl-(7-iodo-6-methyl-hept-6-enyloxy)-dimethyl-silane

: 335455-27-1
(6E,8Z)-8-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methyl-deca-6,8-dien-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / diethyl ether / -78 °C

1.2: diethyl ether / -78 - 0 °C

2.1: 86 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

3.1: 87 percent / PPTS / ethanol / 6 h / 23 °C

With n-butyllithium; potassium hexamethylsilazane; pyridinium p-toluenesulfonate; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1021/ol015667k