N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine

Base Information

Chemical Name:N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine
CAS No.:70517-77-0
Molecular Formula:C₂₆H₄₅NS₂
Molecular Weight:435.782
Hs Code.:

Synonyms:N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine

Chemical Property:

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Technology Process of N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine

There total 4 articles about N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109-80-8
1.3-propanedithiol

: 70517-59-8
p-hexadecylamino benzaldehyde

: 70517-77-0
N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine

Guidance literature:: With magnesium sulfate; zinc(II) chloride; In dichloromethane; for 18h; Ambient temperature;
DOI:10.1021/jm00364a010

Reference yield:

: 69001-50-9
p-(hexadecylamino)benzonitrile

: 70517-77-0
N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / diisobutylaluminum hydride / toluene / 1 h / Ambient temperature

2: 60 percent / magnesium sulfate, zinc chloride / CH₂Cl₂ / 18 h / Ambient temperature

With diisobutylaluminium hydride; magnesium sulfate; zinc(II) chloride; In dichloromethane; toluene;
DOI:10.1021/jm00364a010

Reference yield:

: 112-82-3
hexadecanyl bromide

: 70517-77-0
N-<4-(1,3-dithian-2-yl)phenyl>hexadecylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / HMPA / 22 h / 120 °C

2: 58 percent / diisobutylaluminum hydride / toluene / 1 h / Ambient temperature

3: 60 percent / magnesium sulfate, zinc chloride / CH₂Cl₂ / 18 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; diisobutylaluminium hydride; magnesium sulfate; zinc(II) chloride; In dichloromethane; toluene;
DOI:10.1021/jm00364a010