(5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)

Base Information

Chemical Name:(5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)
CAS No.:916747-75-6
Molecular Formula:C₄₀H₄₀N₆O₂S₂
Molecular Weight:700.929
Hs Code.:

Synonyms:(5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)

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Chemical Property of (5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)

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Technology Process of (5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)

There total 1 articles about (5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 145693-89-6
3-phenyl-(5Z)-5-(pyridine-2-ylmethylene)-2-thioxoimidazolin-4-one

: 4101-68-2
1,10-dibromodecane

: 916747-75-6
(5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at -10 - 20 ℃; for 4h;
DOI:10.1007/s11172-006-0092-7

Reference yield: 80.0%

: 916747-75-6
(5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)

: cobalt(II) chloride hexahydrate

: (5Z,5'Z)-2.2'-(decane-1,10-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)dicobalt(II) tetrachloride dihydrate

Guidance literature:: In ethanol; dichloromethane; EtOH was carefully added to soln. of ligand in CH2Cl2; soln. of Co salt in EtOH was slowly added; mixt. was tightly closed and kept until ppt. was formed; ppt. filtered off; dried (air); elem. anal.;
DOI:10.1007/s11172-006-0092-7