Technology Process of C57H32F10N6O5S
There total 6 articles about C57H32F10N6O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide; 5-(pentafluorophenyl)dipyrromethane;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
at 20 ℃;
for 7h;
Inert atmosphere;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1002/cssc.201200572
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / acetone / 2 h / 60 °C / Inert atmosphere
1.2: 48 h / Reflux; Inert atmosphere
2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere
3.1: acetone / 20 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
5.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 20 °C / Inert atmosphere
6.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
6.2: 7 h / 20 °C / Inert atmosphere
6.3: 0.5 h / 20 °C / Inert atmosphere
With
N-Bromosuccinimide; 2-chloro-1-methyl-pyridinium iodide; potassium carbonate; triethylamine; trifluoroacetic acid; dibenzoyl peroxide;
In
tetrachloromethane; dichloromethane; acetone;
DOI:10.1002/cssc.201200572
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetone / 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
3.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 20 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
4.2: 7 h / 20 °C / Inert atmosphere
4.3: 0.5 h / 20 °C / Inert atmosphere
With
2-chloro-1-methyl-pyridinium iodide; triethylamine; trifluoroacetic acid;
In
dichloromethane; acetone;
DOI:10.1002/cssc.201200572