5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Base Information

Chemical Name:5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine
CAS No.:1427462-38-1
Molecular Formula:C₄₃H₄₇N₃O₁₉
Molecular Weight:909.855
Hs Code.:

Synonyms:5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

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Chemical Property of 5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

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Technology Process of 5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

There total 11 articles about 5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 135253-84-8,60515-61-9
4-aminophenyl-2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-2,3,6-tetra-O-acetyl-β-D-glucopyranoside

: 140447-00-3
2,2'-bipyridine-5-carbonyl chloride

: 1427462-38-1
5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.tet.2013.01.095

Reference yield:

: C₁₄H₂₄O₁₂

: 1427462-38-1
5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 20 °C

2: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C

3: acetone / Reflux

4: hydrogen; palladium on activated charcoal / tetrahydrofuran / 20 °C

5: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

With pyridine; palladium on activated charcoal; hydrogen bromide; hydrogen; acetic anhydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.tet.2013.01.095

Reference yield:

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-glucose pentaacetate

: 1427462-38-1
5-(-N-(p-O-(2,3,6,2,3,4,6-Hepta-O-acetyl-β-lactosyl)phenyl)-aminocarbonyl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 4 steps

1: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C

2: acetone / Reflux

3: hydrogen; palladium on activated charcoal / tetrahydrofuran / 20 °C

4: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

With palladium on activated charcoal; hydrogen bromide; hydrogen; acetic anhydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.tet.2013.01.095