triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

Base Information

Chemical Name:triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide
CAS No.:1373359-69-3
Molecular Formula:C₁₄H₁₉F₃NO₄S*C₁₈H₁₅S
Molecular Weight:617.753
Hs Code.:

Synonyms:triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

Suppliers and Price of triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

There total 4 articles about triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1379583-70-6
N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

: 3353-89-7
triphenylsulfonium bromide

: 1373359-69-3
triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

Guidance literature:: N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide; With sodium hydroxide; In water; at 0 ℃; for 0.5h;

triphenylsulfonium bromide; In chloroform; at 25 - 32 ℃; for 15h; Temperature; Reagent/catalyst;

Reference yield: 87.0%

: 40630-40-8
trifluoromethanesulfonamide ethanol

: 3353-89-7
triphenylsulfonium bromide

: 1373359-69-3
triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

Guidance literature:: trifluoromethanesulfonamide ethanol; With sodium hydroxide; In chloroform; water; at 0 ℃;

triphenylsulfonium bromide; In chloroform; water; at 220 ℃; for 15h;

Reference yield:

: 828-51-3
1-Adamantanecarboxylic acid

: 1373359-69-3
triphenylsulfonium N-[2-(adamantane-1-ylcarbonyloxy)ethyl]trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / toluene / 9 h / Dean-Stark; Reflux

2.1: sodium hydroxide / water / 0.5 h / 0 °C

2.2: 15 h / 25 - 32 °C

With toluene-4-sulfonic acid; sodium hydroxide; In water; toluene;