C₃₁H₃₄N₂O₇

Base Information

Chemical Name:C₃₁H₃₄N₂O₇
CAS No.:1337913-78-6
Molecular Formula:C₃₁H₃₄N₂O₇
Molecular Weight:546.62
Hs Code.:

C<sub>31</sub>H<sub>34</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₁H₃₄N₂O₇

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Chemical Property of C₃₁H₃₄N₂O₇

Chemical Property:

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Technology Process of C₃₁H₃₄N₂O₇

There total 12 articles about C₃₁H₃₄N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₃₇N₂O₈^(1-)*Na⁽¹⁺⁾

: 1337913-78-6
C₃₁H₃₄N₂O₇

Guidance literature:: With dmap; di-tert-butyl dicarbonate; In acetonitrile; at 20 ℃; for 0.333333h;
DOI:10.1021/ol202535f

Reference yield:

: 1337913-90-2
methyl 10-benzyloxy-7-methylene-6-oxo-1,3,4,5,6,7-hexahydroazocino[4,5,6-cd]indole-4-carboxylate

: 1337913-78-6
C₃₁H₃₄N₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / acetonitrile / 0.33 h / 20 °C

2: sodium tri-sec-butylborohydride / tetrahydrofuran / 14 h / -78 - 20 °C

3: dmap; di-tert-butyl dicarbonate / acetonitrile / 0.33 h / 20 °C

With dmap; di-tert-butyl dicarbonate; sodium tri-sec-butylborohydride; In tetrahydrofuran; acetonitrile; 3: Dieckmann reaction;
DOI:10.1021/ol202535f

Reference yield:

: 1337913-86-6
7-benzhydrylindole-3-carboxaldehyde

: 1337913-78-6
C₃₁H₃₄N₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Cooling with ice

1.2: 12 h / 20 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.33 h / 0 °C / Cooling with ice

2.2: 12 h / 20 °C

3.1: Wilkinson's catalyst; hydrogen / methanol; toluene / 50 h / 45 °C / 64645.2 Torr / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

5.1: acetonitrile / 0.5 h / Inert atmosphere; Irradiation

6.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C

7.1: dmap / acetonitrile / 0.33 h / 20 °C

8.1: sodium tri-sec-butylborohydride / tetrahydrofuran / 14 h / -78 - 20 °C

9.1: dmap; di-tert-butyl dicarbonate / acetonitrile / 0.33 h / 20 °C

With dmap; Wilkinson's catalyst; di-tert-butyl dicarbonate; tetrabutyl ammonium fluoride; hydrogen; sodium tri-sec-butylborohydride; sodium hydride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 2.1: Horner-Wadsworth-Emmons olefination / 2.2: Horner-Wadsworth-Emmons olefination / 5.1: Witkop cyclization / 9.1: Dieckmann reaction;
DOI:10.1021/ol202535f