C₃₉H₄₈N₈O₄

Base Information

Chemical Name:C₃₉H₄₈N₈O₄
CAS No.:1359869-65-0
Molecular Formula:C₃₉H₄₈N₈O₄
Molecular Weight:692.861
Hs Code.:

C<sub>39</sub>H<sub>48</sub>N<sub>8</sub>O<sub>4</sub>

Synonyms:C₃₉H₄₈N₈O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₄₈N₈O₄

Chemical Property:

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Technology Process of C₃₉H₄₈N₈O₄

There total 8 articles about C₃₉H₄₈N₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 1359869-64-9
C₃₉H₄₈N₄O₁₀

: 1359869-65-0
C₃₉H₄₈N₈O₄

Guidance literature:: With ammonium acetate; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 18h; Sealed tube;
DOI:10.1055/s-0039-1690699

Reference yield:

: 1359869-61-6
C₁₇H₁₄N₂O₅

: 1359869-65-0
C₃₉H₄₈N₈O₄

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; acetic acid / palladium on activated charcoal / methanol / 2 h / 20 °C

2: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

3: N-ethyl-N,N-diisopropylamine / potassium iodide / acetonitrile / 2 h / 0 - 20 °C

4: ammonium acetate / xylene / 18 h / 130 °C / Inert atmosphere; Sealed tube

With ammonium acetate; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium on activated charcoal; potassium iodide; In tetrahydrofuran; methanol; acetonitrile; xylene;

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 1359869-65-0
C₃₉H₄₈N₈O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: ammonia / zinc trifluoromethanesulfonate / tetrahydrofuran / 0 °C

1.2: 1 h / 0 - 20 °C

1.3: 2 h / Reflux

2.1: benzene / 4 h / 95 °C

3.1: hydrogen; acetic acid / palladium on activated charcoal / methanol / 2 h / 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

5.1: N-ethyl-N,N-diisopropylamine / potassium iodide / acetonitrile / 2 h / 0 - 20 °C

6.1: ammonium acetate / xylene / 18 h / 130 °C / Inert atmosphere; Sealed tube

With ammonium acetate; ammonia; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium on activated charcoal; zinc trifluoromethanesulfonate; potassium iodide; In tetrahydrofuran; methanol; acetonitrile; xylene; benzene;