(1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

Base Information

Chemical Name:(1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate
CAS No.:1309852-42-3
Molecular Formula:C₃₂H₅₁NO₄Si
Molecular Weight:541.847
Hs Code.:

Synonyms:(1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

Suppliers and Price of (1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

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Chemical Property of (1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

Chemical Property:

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Technology Process of (1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

There total 3 articles about (1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-80-0
pent-4-enoic acid

: C₂₂H₃₉NO₂Si

: 1309852-42-3
(1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2011.01.134

Reference yield:

: C₂₂H₃₇NO₂Si

: 1309852-42-3
(1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 1 h / 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

With dmap; sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.01.134

Reference yield:

: 313279-15-1
4-((triisopropylsilyloxy)methyl)benzaldehyde

: 1309852-42-3
(1S,2S)-2-(N-(4-((triisopropylsilyloxy)methyl)benzyl)pent-4-enamido)cyclopentyl pent-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate; triethylamine / dichloromethane / 3 h / 20 °C

2: sodium tetrahydroborate / ethanol / 1 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

With dmap; sodium tetrahydroborate; magnesium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.01.134