2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

Base Information

Chemical Name:2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide
CAS No.:120225-77-6
Molecular Formula:C₂₃H₂₉N₇O₄
Molecular Weight:467.528
Hs Code.:

Synonyms:2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

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Chemical Property of 2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

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Technology Process of 2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

There total 6 articles about 2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1195939-25-3
2-fluoro-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

: 64-04-0
phenethylamine

: 120225-77-6
2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; at 70 ℃; for 168h;
DOI:10.1021/jm300206u

Reference yield:

: 24639-06-3
((3aR,4R,6R,6aR)-6-(6-amino-2-chloro-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol

: 120225-77-6
2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / aq. KOH, KMnO₄ / H₂O / 72 h

2: SOCl₂ / dimethylformamide / 2 h / 50 °C

3: CH₂Cl₂ / 1 h / Ambient temperature

4: 3 h / 130 °C

With potassium hydroxide; potassium permanganate; thionyl chloride; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00169a015

Reference yield:

: 72209-19-9
2-chloro-2',3'-O-isopropylideneadenosine-5'-carboxylic acid

: 120225-77-6
2-(2-phenyl)ethylamino-2',3'-O-isopropylideneadenosine-5'-N-ethylcarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / dimethylformamide / 2 h / 50 °C

2: CH₂Cl₂ / 1 h / Ambient temperature

3: 3 h / 130 °C

With thionyl chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00169a015