didurylketimine

Base Information

Chemical Name:didurylketimine
CAS No.:156746-72-4
Molecular Formula:C₂₁H₂₇N
Molecular Weight:293.452
Hs Code.:

Synonyms:didurylketimine

Suppliers and Price of didurylketimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of didurylketimine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of didurylketimine

There total 1 articles about didurylketimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2571-53-1
2,3,5,6-tetramethylbenzonitrile

: 1646-53-3
bromodurene

: 156746-72-4
didurylketimine

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) diethyl ether, n-hexane, reflux, 2.) diethyl ether, n-hexane, reflux, overnight;
DOI:10.1021/ja9635903

Reference yield:

: 156746-72-4
didurylketimine

: C₂₁H₂₆N₂O

Guidance literature:: With dinitrogen tetraoxide;

Reference yield:

: 156746-72-4
didurylketimine

: 2,3,5-Trimethyl-8-(2,3,5,6-tetramethyl-phenyl)-bicyclo[4.2.0]octa-1⁽⁶⁾,2,4-triene

Guidance literature:: Multi-step reaction with 3 steps

1: N₂O₄, sodium acetate / CCl₄ / 1 h / 5 - 10 °C

2: LiAlH₄ / diethyl ether / -30 - -10 °C

3: benzene / 0 °C / Irradiation

With lithium aluminium tetrahydride; sodium acetate; dinitrogen tetraoxide; In tetrachloromethane; diethyl ether; benzene;
DOI:10.1021/ja9635903