3-duetero-4-iodoanisole

Base Information

• Chemical Name: 3-duetero-4-iodoanisole
• CAS No.: 35776-38-6
• Molecular Formula: C₇H₈O
• Molecular Weight: 109.132
• Mol file: 35776-38-6.mol

Synonyms:3-duetero-4-iodoanisole

Chemical Property of 3-duetero-4-iodoanisole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-duetero-4-iodoanisole

There total 8 articles about 3-duetero-4-iodoanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

3-methoxyphenyl bromide (2398-37-0) → 3-duetero-4-iodoanisole (35776-38-6)

Guidance literature:

With 1,10-Phenanthroline; carbon monoxide; water-d2; copper diacetate; triethylamine; at 140 ℃; for 48h; under 37503.8 Torr;

DOI:10.1039/d1sc04259a

Reference yield:

3-methoxy-1-iodobenzene (766-85-8) → 3-duetero-4-iodoanisole (35776-38-6)

Guidance literature:

With diethyl ether; magnesium; anschliessend Behandeln mit Deuteriumoxid;

DOI:10.1039/jr9560003911

Reference yield:

(3-methoxyphenyl)(triphenyl-λ5-phosphanyl)gold → 3-duetero-4-iodoanisole (35776-38-6)

Guidance literature:

With N-Bromosuccinimide; In benzene-d6; at 20 ℃; regioselective reaction;

DOI:10.1016/j.jorganchem.2008.11.054

upstream raw materials:

3-methoxyphenyl bromide

3-methoxy-1-iodobenzene

methoxybenzene

(3-methoxyphenyl)(triphenyl-λ5-phosphanyl)gold

Downstream raw materials:

para-iodoanisole

Refernces

• 1、 Bartling, Stephan,Beller, Matthias,Bourriquen, Florian,Junge, Kathrin,Li, Wu,Liu, Weiping,Qu, Ruiyang,Rockstroh, Nils. "Copper-catalysed low-temperature water-gas shift reaction for selective deuteration of aryl halides". . p. 14033 - 14038. Retrieved 2021/11/12.
• 2、 Patra, Tuhin,Mukherjee, Satobhisha,Ma, Jiajia,Strieth-Kalthoff, Felix,Glorius, Frank. "Visible-Light-Photosensitized Aryl and Alkyl Decarboxylative Functionalization Reactions". . p. 10514 - 10520. Retrieved 2019/07/12.