Diphenyl-triphenylstannylmethyl-phosphinsulfid

Base Information

Chemical Name:Diphenyl-triphenylstannylmethyl-phosphinsulfid
CAS No.:105022-38-6
Molecular Formula:C₃₁H₂₇PSSn
Molecular Weight:581.305
Hs Code.:

Synonyms:Diphenyl-triphenylstannylmethyl-phosphinsulfid

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Chemical Property of Diphenyl-triphenylstannylmethyl-phosphinsulfid

Chemical Property:

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Technology Process of Diphenyl-triphenylstannylmethyl-phosphinsulfid

There total 4 articles about Diphenyl-triphenylstannylmethyl-phosphinsulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 52101-86-7
lithium methylenediphenylthiophosphinate

: 639-58-7
triphenyltin chloride

: 105022-38-6
Diphenyl-triphenylstannylmethyl-phosphinsulfid

Guidance literature:: In tetrahydrofuran; diethyl ether; byproducts: LiCl; under Ar; a soln. of LiCH2PSPh2 in THF/Et2O was cooled with a dry ice/acetone mixt., addn. of the Sn compd., stirred for 15 min, warmed to room temp.; concd. under reduced pressure, addn. of Et2O, filtered, washed with Et2O, dried in vac.;
DOI:10.1016/S0277-5387(00)80101-1

Reference yield:

: 42393-72-6
(C₆H₅)3SnCH₂CH₂N(CH₃)C₆H₅

: 105022-38-6
Diphenyl-triphenylstannylmethyl-phosphinsulfid

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / diethyl ether

2: diethyl ether; tetrahydrofuran

With HCl; In tetrahydrofuran; diethyl ether;

Reference yield:

: 42393-74-8
(C₆H₅)3SnCH₂CH₂N(C₆H₅)2

: 105022-38-6
Diphenyl-triphenylstannylmethyl-phosphinsulfid

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / diethyl ether

2: diethyl ether; tetrahydrofuran

With HCl; In tetrahydrofuran; diethyl ether;