C₁₅H₂₂OS

Base Information

• Chemical Name: C₁₅H₂₂OS
• CAS No.: 1332505-58-4
• Molecular Formula: C₁₅H₂₂OS
• Molecular Weight: 250.405
• Mol file: 1332505-58-4.mol

Synonyms:C₁₅H₂₂OS

Chemical Property of C₁₅H₂₂OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₅H₂₂OS

There total 2 articles about C₁₅H₂₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(E)-S-butyl 5-phenylpent-2-enethioate (1332505-48-2) → C15H22OS (1332505-58-4)

Guidance literature:

With copper acetate monohydrate; o-phenylenebis(diphenylphosphine); tert-butyl alcohol; In toluene; at 20 ℃; for 5h; chemoselective reaction; Inert atmosphere;

DOI:10.1039/c1ob05352c

Reference yield:

5-phenyl-2(E)-pentenoic acid (24271-22-5,55320-96-2,138034-94-3) → C15H22OS (1332505-58-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: copper acetate monohydrate; o-phenylenebis(diphenylphosphine); tert-butyl alcohol / toluene / 5 h / 20 °C / Inert atmosphere

With dmap; copper acetate monohydrate; o-phenylenebis(diphenylphosphine); 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tert-butyl alcohol; In dichloromethane; toluene;

DOI:10.1039/c1ob05352c

upstream raw materials:

(E)-S-butyl 5-phenylpent-2-enethioate

5-phenyl-2(E)-pentenoic acid